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Synthesis of thio
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Synthesis of thio


Date:01.06.2016, 13:18 N -methylimidazole-Et3N and LiOH, and stereoretentive Suzuki-Miyaura cross-coupling. H. Nakatsuji, H. Nishikado, K. Ueno, Y. Tanabe, Org. Lett., 2009, 11,. Pentafluorophenylammonium triflate (PFPAT ) successfully catalyzed the C-acylation of enol silyl ethers with acid chloride to produce various -diketones in good. Abstract Sufentanil, a potent anilidopiperidine analgesic, was synthesized from a simple thio -phenylethylamine via a six step sequence. The key parts of this synthesis involved an efficient construction of thiophenylethylpiperidone by aminomethano desilylation-cyclization followed by Swern oxidation and a direct regioselective. Methylation of piperidylmethanol ( 11 ) was achieved by an initial reaction with diazomethane 6. Finally, the synthesis was completed by the known acylation of anilinopiperidine 12 with propionic anhydride 2 to afford the desired product which was identical in all.
Synthesis of thio


Synthesis of thio Synthesis of thio


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